![bruker apex ii software bruker apex ii software](https://xray.chem.tamu.edu/images/instuments/apexii.jpg)
We still get the same error messages and the goniometer just does not move. We reassembled the goniometer assembly and were hoping that all issues would be resolved and the instrument would start up normally. But, unfortunately the wires connecting the motherboard to the motor and encoder for the kappa and phi axis had gotten so twisted that we needed to replace them.ģ) We obtained new encoder cables from Bruker and managed to replace all the cables. We thought that we had potentially managed to open things up and located the source of the problem. Consequently, it torqued/rotated the wires inside the central part of the goniometer and created a strain/tension in the lines due to which a lot of the wired connections to both the "motor" and the "encoder" to the "Kappa" and "Phi" axis got yanked from their positions. Upon, starting the instrument we encountered the same error and the same problem with no movement of the goniometer.Ģ) Upon further investigation we found that due to issues related to failed limit switches our "Omega" axis rotated more than the prescribed limits for the axis (see attached document called "Kappa Goniometer Issues" for details).
![bruker apex ii software bruker apex ii software](https://blue-scientific.com/wp-content/uploads/apex3-interface-300x165.jpg)
So, we replaced all the limit switches with new ones. Since my last post a lot has happened and I will try and briefly explain all that to you here.ġ) We found broken limit switches at the back of the goniometer assembly and thought that could be a problem. 2015, C71, 3.Dual source instrument equipped with a TRIUMPH monochromated Moly sealed tube and a Copper IµS. System features a Kappa goniometer and a Photon II detector as well as an Oxford Cryosystems Cryostream for variable temperature data collection from 90-400 K.Thanks a ton for your reply.
![bruker apex ii software bruker apex ii software](https://img.directindustry.com/images_di/photo-g/30028-10804205.jpg)
BRUKER 1000 CCD Diffractometer will be the second working device for Single Crystal Structure Determination. Instrument is currently located on the BioSide of campus.
BRUKER APEX II SOFTWARE SOFTWARE
#BRUKER APEX II CCD DETECTOR SOFTWARE#Ĭurrently we are upgrading it with video camera, modern APEX II Software Suite and low-temperature BRUKER LT-3 device.
BRUKER APEX II SOFTWARE GENERATOR
It is equipped with a Copper MicroMax 003f X-ray generator and PILATUS R200K Hybrid Pixel Array Detector as well as an Oxford Cryosystems Cobra for variable temperature data collection from 90-400 K.īruker D8 Venture Diffractometer-Ga MetalJet Most of the time it will be equipped with Cu radiation, however, it can be switched to Mo-radiation if needed. Single crystal diffractometer Bruker 'Kappa APEX DUO'. Instrument is equipped with a Gallium MetalJet source and a Photon III detector as well as an Oxford Cryosystems Cryostream for variable temperature data collection from 90-500 K. The Bruker X8 Apex instrument was installed in 2005.
![bruker apex ii software bruker apex ii software](http://xrd.spbu.ru/netcat_files/122/126/Bruker_Duo.jpg)
Instrument is equipped with a Moly sealed tube and an Apex-II CCD detector as well as an Oxford Cryosystems Cryostream for variable temperature data collection from 90-400 K. Category: Equipment of Centre for X-ray Diffraction Studies.
BRUKER APEX II SOFTWARE SERIES
It is equipped with an Oxford Cryostream series 800 variable temperature unit providing sample temperature from 90 to 400K. It operates with a fine focus sealed tube Mo X-ray source and an APEX II CCD detector. Single-crystal XRD data were collected on a Bruker SMART APEX II CCD X detector using graphite-monochromated Mo KR radiation ( 0.71073 A) and intergrated with the SAINT-Plus program.18 A colorless and transparent crystal with dimen-sions 0.32 30.23 0. Dual source instrument equipped with a TRIUMPH monochromated Moly sealed tube and a Copper IS. A single crystal diffractometer which combines molybdenum and copper X-ray sources with a highly accurate goniometer and the most sensitive CCD detector allowing fast and redundant data collection to high. Instrument is equipped with a Moly rotating anode source and a Photon III detector as well as an Oxford Cryosystems Cryostream for variable temperature data collection from 90-500 K.